BI-AMPEROMETRIC TITRATION PDF

A novel biamperometric methodology for thorium determination by EDTA complexometric titration. Studies carried out showed that a pH range of 2. The present paper describes a simple method based on the determination of U IV and total U by biamperometric titration. A new approach to flow-batch titration. A monosegmented flow titrator with coulometric reagent generation and potentiometric or biamperometric detection. Monosegmented flow analysis MSFA has been used as a flow-batch system to produce a simple, robust, and mechanized titrator that enables true titrations to be performed without the use of standards.

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Published on Jun 18, Amperometry refers to the measurement of current under a constant applied voltage and under these conditions it is the concentration of analyte which determine the magnitude of current. In Amperometric titrations, the potential applied between the indicator electrode dropping mercury electrode and the appropriate depolarizing reference electrode saturated calomel electrode is kept constant and current through the electrolytic cell is then measured on the addition of each increment of titrating solution.

It is a form of quantitative analysis. Otherwise called as Polarographic or polarometric titrations. SlideShare Explore Search You. Submit Search. Successfully reported this slideshow.

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Embeds 0 No embeds. No notes for slide. Amperometric Titrations 1. Amperometric Titrations DR. So, if some of the electroactive material in the solution is removed by interaction with some other reagent the diffusion current will decrease proportionally. Diameter of 0. You just clipped your first slide!

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Amperometric titration

Amperometric titration refers to a class of titrations in which the equivalence point is determined through measurement of the electric current produced by the titration reaction. It is a form of quantitative analysis. A solution containing the analyte, A, in the presence of some conductive buffer. If an electrolytic potential is applied to the solution through a working electrode, then the measured current depends in part on the concentration of the analyte. Measurement of this current can be used to determine the concentration of the analyte directly; this is a form of amperometry. However, the difficulty is that the measured current depends on several other variables, and it is not always possible to control all of them adequately.

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Biamperometric end-point determination in the titration of fluoride with thorium nitrate

We'd like to understand how you use our websites in order to improve them. Register your interest. Die Anwendung verschiedener identischer Elektrodenpaare wurde untersucht. The possibilities of the biamperometric end-point detection in the titration of fluoride by means of thorium nitrate are investigated applying different pairs of identical indicator electrodes. In unbuffered solutions using aluminium, bismuth and tin pairs of polarised indicator electrodes, amounts of 6.

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Slideshare uses cookies to improve functionality and performance, and to provide you with relevant advertising. If you continue browsing the site, you agree to the use of cookies on this website. See our User Agreement and Privacy Policy. See our Privacy Policy and User Agreement for details. Published on Jun 18, Amperometry refers to the measurement of current under a constant applied voltage and under these conditions it is the concentration of analyte which determine the magnitude of current. In Amperometric titrations, the potential applied between the indicator electrode dropping mercury electrode and the appropriate depolarizing reference electrode saturated calomel electrode is kept constant and current through the electrolytic cell is then measured on the addition of each increment of titrating solution.

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